Detection of cassava and sweet potato starch in adulterated lotus root starch by differential scanning calorimetry
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摘要: 为了对掺入藕粉中的其他淀粉种类进行鉴别,本研究通过差示扫描量热仪对藕粉等常见几种淀粉的糊化过程进行考察发现,藕粉与其他淀粉在糊化吸热峰上有着明显的差别。根据藕粉与木薯淀粉和甘薯淀粉等在糊化吸热峰上的差异,以糊化吸热峰作为特征指标,对掺假藕粉中掺入的木薯淀粉和甘薯淀粉进行定性或定量鉴别实验。同理,此方法也可用于检验与藕粉在糊化吸热峰上有明显差异的用于藕粉掺假的其他淀粉种类,如马铃薯淀粉,玉米淀粉等。此方法将弥补前期发表的基于淀粉颗粒超微形貌特征的可食用淀粉种类扫描电镜鉴别方法的不足。Abstract: To detect other starch adulterated in lotus root starch product, gelatinization process of lotus root starch and other 7 kinds of common edible starch were analyzed through differential scanning calorimetry ( DSC) .According to the difference of gelatinization endothermal peak among lotus roots, cassava and sweet potato starch, a DSC method was developed to detect the added cassava and sweet potato starch in false lotus root starch product qualitatively and quantitatively based on the presence and the height of gelatinization endothermal peak of cassava or sweet potato starch. Additionally, this method was also valid in the detection of other starch adulterated in lotus root starch product, such as potato and corn starch etc., of which the endothermal peaks of gelatinization were different from that of lotus root starch.This method is a supplement for the SEM method, which had been developed to differentiate various edible starches in our previous research.
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[1] 王振莲, 赵琦, 李承森, 等.古莲的研究现状[J].北京师范大学学报, 2005, 26 (2) :55-58. [2] 陈咏梅, 高盐生.藕淀粉特性的研究[J].盐城工业学院学报, 1999, 12 (3) :67-71. [3] 闵燕萍, 陈宗道, 钟耕, 等.藕淀粉的加工性能研究[J].农业工程学报, 2007, 23 (1) :259-263. [4] 秦志荣, 许荣年, 汪庆旗, 等.藕淀粉颗粒性质的研究及藕粉产品的鉴定[J].食品与发酵工业, 2005, 31 (1) :136-138. [5] SUZUKI A, KANEYAMA M, SHIBANUMA K, et al.Characterization of lotus starch[J].Cereal Chemistry, 1992, 69:309-315.
[6] 李良俊, 张晓冬, 沈新平, 等.莲藕淀粉RVA谱特征和淀粉粒形态的研究[J].园艺学报, 2006, 33 (3) :534-538. [7] 王绍清, 武士奎, 穆同娜, 等.扫描电镜和稳定碳同位素比质谱法鉴别马铃薯淀粉中的掺假玉米淀粉[J].食品科学, 2010 (31) :332-335. [8] 王绍清, 王琳琳, 范文浩, 等.扫描电镜法分析常见可食用淀粉颗粒的超微形貌[J].食品科学, 2011, 32 (15) :74-75. [9] 王绍清, 王琳琳, 范文浩, 等.扫描电子显微镜法原位观察可食用淀粉颗粒的超微形貌[J].食品科学, 2013, 34 (1) :61-64. [10] 赵凯, 等.食品淀粉的结构、功能及应用[M].第4章淀粉结构与功能.书名原文:Starch in Food:Structure, Function and Applications, edited by ELIASSON AC.赵凯, 等译, 2009, 中国轻工业出版社, 北京. [11] 顾正彪.DSC在淀粉研究中的应用[J].无锡轻工大学学报, 1996, 15 (2) :179-182. [12] (日) 二国二郎.淀粉科学手册[M].北京:中国轻工业出版社, 1989. [13] 项丽霞, 田翠华, 李洁, 等.莲藕淀粉糊化温度的测定[J].食品工业科技, 2006, 27 (2) :63-64. [14] 闵燕萍, 陈宗道, 钟耕, 等.藕淀粉的加工性能研究[J].农业工程学报, 2007, 27:259-263. [15] 秦志荣, 许荣年, 汪庆旗, 等.藕淀粉颗粒性质的研究及藕粉产品的鉴定[J].食品与发酵工业, 2005, 31 (1) :136-138. [16] 高群玉, 吴磊, 刘kun.甘薯淀粉糊性质的研究[J].食品工业科技, 2008, 29 (8) :153-155. [17] 谭洪卓, 谭斌, 刘明, 等.甘薯淀粉性质与其粉丝品质的关系[J].农业工程学报, 2009, 25 (4) :286-292. [18] COLLADO LS, MABESA RG, CORKE H.Genetic variation in the physical properties of sweet potato starch[J].Journal of Agricultural and Food Chemistry, 1999, 47:4195-4201.
[19] DEFLOOR I, DEHING I, DELCOUR JA.Physicochemical properties of cassava starch[J].Starch/Strke, 1999, 50:58-64.
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